材料科学与工程

妥尔油酸二乙醇酰胺水基润滑添加剂的摩擦学性能

  • 何红坤 ,
  • 于桂峰 ,
  • 郝延龙 ,
  • 常 青 ,
  • 严志军 ,
  • 朱新河 ,
  • 程 东
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  • (大连海事大学 轮机工程学院, 辽宁 大连 116026)
何红坤(1988—),男,硕士生.

收稿日期: 2015-06-29

  修回日期: 2015-09-08

  网络出版日期: 2015-09-09

Tribological performance of the tall oleic acid diethanolamide water based lubricant additive

  • HE Hong-kun ,
  • YU Gui-feng ,
  • HAO Yan-long ,
  • CHANG Qing ,
  • YAN Zhi-jun ,
  • ZHU Xin-he ,
  • CHENG Dong
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  • (Marine Engineering College,Dalian Maritime University, Dalian 116026, China)

Received date: 2015-06-29

  Revised date: 2015-09-08

  Online published: 2015-09-09

摘要

以精制妥尔油和二乙醇胺为主要原料合成妥尔油酸二乙醇酰胺,考察在原料摩尔配比为1∶1的混合条件下所生成的该类水基润滑添加剂的摩擦学性能.采用四球摩擦磨损试验机考察不同浓度添加剂极压、减磨性能;参照GB-T6144-2010对其pH、防锈性能进行测定.结果表明:妥尔油酸二乙醇酰胺可以极大提高水基极压性能,5%润滑液PB值高达1020 N;随着浓度增高,减磨特性增强, pH满足国标要求;浓度增加至3%后,防锈性能达到A级.

本文引用格式

何红坤 , 于桂峰 , 郝延龙 , 常 青 , 严志军 , 朱新河 , 程 东 . 妥尔油酸二乙醇酰胺水基润滑添加剂的摩擦学性能[J]. 大连海事大学学报, 2016 , 42(1) : 125 -128 . DOI: 10.16411/j.cnki.issn1006-7736.2016.01.022

Abstract

Tall oleic acid diethanolamide was synthesized from refined tall oil and diethanolamine as main raw material mixed, and the tribological performance of its waterbased lubricant additive produced by mixing with molar ratio of 1∶1 was studied. The behaviors of extreme pressure and anti-attrition for different concentrations of additives were examined by testing on a four-ball tester, and the pH value and rust protection performance were measured according to GB-T6144-2010. Results show that water base extreme pressure performance can be improved by using tall oleic acid diethanolamide, and PB value is up to 1020 N for 5% lubricant, the higher concentration, the better the antifriction performance. pH meets the requirements of national standard, and rust protection reaches to A level as concentration up to 3%.

参考文献

[1]KOSKI A.Applicability of crude tall oil for wood protection faculty of technology[D].Oulu,Finland:University of Oulu,2008.
[2]HYVÖNEN A,NELO M,PILTONEN P,et al.Using iron catalyst to enhance the drying properties of crude tall oil-based wood preservative[J]. Holz als Roh-und Werkstoff,2007,65(2):105-111.
[3]杨兴明.自生压合成妥尔油二聚脂肪酸的工艺研究[J].广东化工,1995(1):20-23.
YANG Xing-ming.The study of Autogenic pressure tall oil dimer fatty acid synthesis technology[J].Guangdong Chemical Industry,1995(1):20-23.(in Chinese)
[4]李宏,涂政文,付尚发,等.妥尔油酸铜与ZDDP复配物的摩擦学性能研究[J].武汉化工学院学报,2001,23(3):58-59.
LI Hong,TU Zheng-wen,FU Shang-fa,et al.A Tribologic study of compound of cupric tailolate and zinc dialkyl dithiophosphate[J].Journal of Wuhan Institute of Chemical Technology,2001,23(3):58-59.(in Chinese)
[5]钟明.磺化妥尔油酸胺的合成及润滑防锈性能研究[J].化工技术与开发,2011,40(5):11-12.
ZHONG Ming.Synthesis of sulfonated tall oil ammonium oleate and its antirust lubrication performance research[J].Technology & Development of Chemical Industry,2011,40(5):11-12.(in Chinese)
[6]吕俊凡,黄奋,钟明.妥尔油酸二乙醇酰胺的合成及其润滑防锈性能研究[J].化工技术与开发,2013,42(10):17-18.
LV Jun-fan,HUANG Fen,ZHONG Ming.Synthesis and antirust performance study on tall oil acid diethanolamide[J].Technology & Development of Chemical Industry,2013,42(10):17-18.(in Chinese)
[7]杨宏,陈战.铜拉丝润滑关键技术研究[J].润滑与密封,2012,37(7):106-108.
YANG Hong,CHEN Zhan.Research on the key technology of copper wire drawing lubrication[J].Lubrication Engineering,2012,37(7):106-108.(in Chinese)
[8]刘喜梅,罗新民.水基润滑添加剂的理论及应用[J].合成润滑材料,2001,28(1):9-13.
LIU Xi-mei,LUO Xin-min.The theory and application of water-based lubricating additives[J].Synthetic Lubricants,2001,28(1):9-13.(in Chinese)
[9]温诗铸,黄平.摩擦学原理[M].第3版.北京:清华大学出版社,2008:5.
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