大连海事大学学报 >
2021 , Vol. 47 >Issue 3: 120 - 124
DOI: https://doi.org/10.16411/j.cnki.issn1006-7736.2021.03.015
基于微电子喷墨打印法制备Li4Ti5O12电极及其电化学性能
收稿日期: 2021-02-05
修回日期: 2021-05-31
网络出版日期: 2021-05-31
基金资助
大连市科技创新基金资助项目(2018J12GX053).
#br# Preparation and electrochemical properties of Li4Ti5O12electrode based on microelectronic ink jet printing
Received date: 2021-02-05
Revised date: 2021-05-31
Online published: 2021-05-31
杨柳 , 张莉 , 崔亚军 , 杜晓梅 , 黄乃宝 , 阎景旺 . 基于微电子喷墨打印法制备Li4Ti5O12电极及其电化学性能[J]. 大连海事大学学报, 2021 , 47(3) : 120 -124 . DOI: 10.16411/j.cnki.issn1006-7736.2021.03.015
In order to solve the problems of complicated operation and high cost existing in traditional preparation technology, the pure phase lithium titanate (LTO) / copper foil (Cu) thin film electrode without adhesive was successfully prepared by microelectronic ink jet printing combined with high temperature annealing. Scanning electron microscope analysis results show that the pure phase LTO with nanoparticle shape can be uniformly deposited on the surface of Cu. The button cell assembled with 10 layers of active material LTO / Cu film electrode and Li negative electrode by inkjet printing has a specific capacity of 91.27 mA·h/g at 3C (1.0 ~ 1.7 V) current density, and after 1000 cycles, the retention rate of discharge specific capacity is 85.4%, which show excellent cycle stability. The above results show that the method of inkjet printing combined with high temperature annealing has a broad application prospect in the preparation of electrode materials without adhesive.
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